绿豆淀粉/纤维素纳米晶胶囊壳的制备及表征
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作者单位:

(1.长沙理工大学化学化工学院 长沙 410076;2.长沙理工大学食品与生物工程学院 长沙 410076)

作者简介:

陈启杰(1980—),男,博士,教授 E-mail: chenqijie@126.com

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基金项目:

科技部基础资源研究项目(2019FY100900);湖南省自然科学基金项目(2020JJ4095);湖南省企业科技创新创业团队项目(201918);湖南省高新技术产业科技创新引领计划项目(2021GK4040)


Preparation and Characterization of Mung Bean Starch / Cellulose Nanocrystals Capsules
Author:
Affiliation:

(1.School of Chemistry and Chemical Engineering, Changsha University of Science and Technology, Changsha 410076;2.School of Food Science and Bioengineering, Changsha University of Science and Technology, Changsha 410076)

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    摘要:

    以绿豆淀粉(MBS)和纤维素纳米晶(CNC)为原料,辅以甘油和卡拉胶作为增塑剂和胶凝剂,通过流延法和浸渍法分别制备MBS/CNC胶囊膜和其对应的胶囊壳,并采用傅里叶变换红外光谱(FT-IR)、X射线衍射(XRD)、扫描电子显微镜(SEM)对其进行表征。结果表明,CNC能够有效增强MBS基胶囊壳的拉伸强度,当CNC用量为6.0%时,绿豆淀粉基胶囊膜的拉伸强度为15.61 MPa,提高了175.2%。MBS/CNC胶囊壳的透明度随CNC用量的增加而略微下降。MBS/CNC胶囊壳的干燥失重率在14.14%~14.99%之间,且在蒸馏水和模拟人工胃液中的崩解时限为14 min内,均符合《中国药典》(2015)的规定要求。

    Abstract:

    The starch based capsules were prepared with mung bean starch (MBS) and cellulose nanocrystals (CNC), the glycerol and carrageenan were used as plasticizer and gelling agents. The MBS/CNC capsule-film was prepared by casting method, and the dipping method was used in preparation of the corresponding capsules. The MBS/CNC capsules were analyzed by FTIR, XRD, and SEM. The results showed that CNC could significantly improve the tensile strength of the MBS based capsule. When the content of CNC was 6.0%, the tensile strength of the capsule-film was 15.61 MPa and increased by 175.2%. The transparency of the capsule with different CNC contents was slightly reduced. The loss on drying of the MBS/CNC capsules were between 14.14% and 14.99%, and the disintegration time in distilled water and simulated artificial gastric juice were less than 14 min, which all met the requirements of Chinese Pharmacopoeia (2015).

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陈启杰,赵雅兰,踪张扬,张朋,王凤,谢琼华,王建辉.绿豆淀粉/纤维素纳米晶胶囊壳的制备及表征[J].中国食品学报,2022,22(8):182-189

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  • 收稿日期:2021-08-12
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  • 在线发布日期: 2022-09-08
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