海豹油Pickering乳液的制备及其稳定性研究
作者:
作者单位:

(1.浙江工商大学海洋食品研究院 浙江省水产品加工技术研究联合重点实验室海洋食品精深加工关键技术省部共建协同创新中心 杭州 310012;2.浙江树人大学生物与环境工程学院 杭州 310015)

作者简介:

通讯作者:

中图分类号:

基金项目:

浙江省自然科学基金项目(LQ22C200008,LQ22 C200010);国家重点研发计划课题(2023YFD 2100004)


Studies on the Preparation and Stability of Seal Oil Pickering Emulsion
Author:
Affiliation:

(1.Collaborative Innovation Center of Seafood Deep Processing, Zhejiang Province Joint Key Laboratory of Aquatic Products Processing, Institute of Seafood, Zhejiang Gongshang University, Hangzhou 310012;2.College of Biology and Environmental Engineering, Zhejiang Shuren University, Hongzhou 310015)

Fund Project:

  • 摘要
  • |
  • 图/表
  • |
  • 访问统计
  • |
  • 参考文献
  • |
  • 相似文献
  • |
  • 引证文献
  • |
  • 资源附件
  • |
  • 文章评论
    摘要:

    为制备海豹油Pickering乳液并研究其稳定性,研究了不同稳定剂(酪蛋白酸钠、卵磷脂、β-环糊精)及添加量(1,2,3,4,5 g/100 mL),不同油相体积分数(40%,50%,60%,70%,80%)对乳液特征指标(黏度、静置乳化指数、离心稳定性、粒径)的影响,初步确定了海豹油Pickering乳液的制备工艺,而后通过乳液的外观及显微变化、粒径变化和离心稳定性的变化评价乳液的巴氏杀菌稳定性(65 ℃/30 min,72 ℃/15 s)、冻融稳定性(-18 ℃冷冻24 h,25 ℃下解冻)和贮藏稳定性(25 ℃/28 d)。结果表明:在β-环糊精为稳定剂,油相体积分数为70%,稳定剂添加量为4 g/100 mL的条件下,制得海豹油Pickering乳液,乳液的粒径15.31 μm、离心稳定性86.73%。巴士杀菌处理对乳液特性的影响较小,其中72 ℃/15 s热处理对乳液特性的影响小于65 ℃/30 min时的。冻融显著影响乳液特性,冻融后乳液失稳,油水分离,不再呈现乳液的特性。25 ℃条件下贮藏28 d,乳液虽出现粒径增大、离心稳定性下降等现象,但仍保持了基本特性。结论:以β-环糊精为稳定剂可以制得海豹油Pickering乳液,该乳液具备较好的热稳定性和贮藏稳定性(28 d内),而不具备冻融稳定性。

    Abstract:

    In order to prepare seal oil Pickering emulsion and study its stability, different stabilizers (sodium caseinate, lecithin and β-cyclodextrin), different oil volume fractions (40%, 50%, 60%, 70%, and 80%), and different stabilizer dosages (1, 2, 3, 4, 5 g/100 mL) on the characteristics of the emulsion (viscosity, standing emulsification index, centrifugal stability and particle size) were studied and the preparation process of seal oil Pickering emulsion were preliminarily determined. Then, the pasteurization stability (65 ℃/30 min, 72 ℃/15 s), freeze-thaw stability (freezing at -18 ℃ for 24 h, thawing at 25 ℃) and storage stability (25 ℃/28 d) were evaluated by the appearance and microscopic changes, particle size and centrifugation stability of the emulsion. The results showed that under the conditions of β-cyclodextrin as stabilizer, the oil volume fractions was 70%, and the amount of stabilizer was 4 g/100 mL, seal oil Pickering emulsion could be prepared, and the particle size and centrifugal stability of the emulsion were 15.31 μm and 86.73%, respectively. The effect of pasteurization treatment on the characteristics of the emulsion was not obvious, and the effect of treatment at 72 ℃/15 s on the characteristics of the emulsion was less than 65 ℃/30 min. The freeze-thaw treatment significantly affected the emulsion, and after freeze-thaw, the emulsion was unstable, the oil phase and water phase was separated, and the characteristics of the emulsion were no longer present. Within 28 days of storage at 25 ℃, although the particle size of the emulsion increased and the centrifugation stability decreased, the basic characteristics of the emulsion were maintained. In short, seal oil Pickering emulsion could be prepared by β-cyclodextrin, which has good thermal stability and storage stability (within 28 days), but freeze-thaw stability.

    参考文献
    相似文献
    引证文献
引用本文

郑振霄,董烨,杨加成,徐雪姣.海豹油Pickering乳液的制备及其稳定性研究[J].中国食品学报,2024,24(9):226-233

复制
分享
文章指标
  • 点击次数:
  • 下载次数:
  • HTML阅读次数:
  • 引用次数:
历史
  • 收稿日期:2023-09-22
  • 最后修改日期:
  • 录用日期:
  • 在线发布日期: 2024-10-21
  • 出版日期:
文章二维码
版权所有 :《中国食品学报》杂志社     京ICP备09084417号-4
地址 :北京市海淀区阜成路北三街8号9层      邮政编码 :100048
电话 :010-65223596 65265375      电子邮箱 :chinaspxb@vip.163.com
技术支持:北京勤云科技发展有限公司

漂浮通知


×
《中国食品学报》杂志社招聘编辑