Non-target Screening of Pesticide Residues in Herbal Tea by Gas Chromatography-Quadrupole-Time of Flight Mass Spectrometry
CSTR:
Author:
Affiliation:

(Guangzhou Customs Technology Center, Guangzhou 510623)

Clc Number:

Fund Project:

  • Article
  • |
  • Figures
  • |
  • Metrics
  • |
  • Reference
  • |
  • Related
  • |
  • Cited by
  • |
  • Materials
  • |
  • Comments
    Abstract:

    A method for rapid screening of pesticide residues in herbal tea by gas chromatography coupled with quadrupole time-of-flight mass spectrometry (GC-Q-TOF/MS) was developed. The target compounds in samples were extracted by ethyl acetate, cleaned by GCB and NH2 sorbent and determined by GC-Q-TOF/MS. The detection limits of 20 controlled pesticides were within 2.00-50.0 μg/kg and the limits of quantitation were 5.0-150 μg/kg. The average recovery of the sample ranged from 73.47%-106.3% at three different spiked levels(25, 50, 125 μg/kg), with RSDs (n=6) of 0.91%-9.11%. Moreover, the acquired data was compared with the library using the accurate mass of characteristic ion, ratio of product ion and isotopic distribution of characteristic ion to screen pesticide residues in herbal tea. Screening and confirmation was achieved by library search, and the minimum concentration with a score(≥80) was used as the screening limit of the method without reference standards. This method is high efficiency, sensitive and accuracy, and can meet the requirement for non-target rapid screening of pesticide residues in herbal tea.

    Reference
    Related
    Cited by
Get Citation
Share
Article Metrics
  • Abstract:
  • PDF:
  • HTML:
  • Cited by:
History
  • Received:May 17,2021
  • Revised:
  • Adopted:
  • Online: June 15,2022
  • Published:
Article QR Code
Copyright :Journal of Chinese Institute of Food Science and Technology     京ICP备09084417号-4
Address :9/F, No. 8 North 3rd Street, Fucheng Road, Haidian District, Beijing, China      Postal code :100048
Telephone :010-65223596 65265376      E-mail :chinaspxb@vip.163.com
Supported by : Beijing E-Tiller Technology Development Co., Ltd.